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Nanoliters: Fundamentals Of Induction Based Fluidics.

Applications To Sample Preparation/Treatment & Instrument Introduction.

To TLC, MALDI, SPE, IR, LC, SIMS, UV/Vis, ESI,

DART & More.

 

Introduction

Why nanoliters and IBF?. Economics, health, aesthetics & practicality

Traditional/non-traditional fluidic devices considered  

Limitations of pipettes, syringes, mechanical systems

IBF history

                Studying ESI w/Agilent, Affymax and Chem Space to understand ESI

                                Traditional microfluidics contrasted to ESI

                                ESI contrasted to IBF

                                                Other liquid movement approaches addressed and contrasted.

    e.g., Millikan,inkjets; piezo, chips.

 

Example IBF Applications with Video.

Parallel dispensing, parallel LC with tight MALDI sample placement

Million fold dilution, e-spotting, TLC, toxicology chemicals onto animals, NCB sample handling

DNA/RNA prep. Samples fly to humans for dispensing medication.  Others

Demo of the nl/uL Syringe.

 

Moving matter.

              Laminar  flow, capillary action, adhesion and cohesion.

                              Flying matter

    Baseballs, Bullets, Electrons in tubes, Millikan's experiment, Inkjets

              IBF and Mass Spectrometers {ions, gasses, liquids}

                                Forces considered-contrasted. Liquid trajectories calculated

Explaining energy of flying nanoliters in one application

                           Simple explanation of IBF in a capillary

Simple explanation of IBF flying liquids to humans

Simple explanation of parallel IBF dispensing
                                                                                                                                                                                    
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Instrumentation: The Nanoliter Syringe, The Nanoliter Pipette, The Nanoliter Pumps

                Liquid transport specification (Simple or complex task.)

                Plumbing, manifold or chip considerations

                Energy sources

Electrokinetic

Pneumatic, peristaltic, ultrasonic, other for hybrid systems

Robotic considerations

Interface/s

Detection

 

Practical issues in liquid transport, across the macro, micro and nano regimes.

Evaporation after Maxwell

Electrochemistry after Adams/Bard.

Particles

Viscosity

Surfaces Energy

Joule heating

Environmental factors

Non ideal consideration in nanofluidics briefly considered

New Publications. 

Calibration

               Approaches

Photoshop/Paintshop Pro demo

               Calibration software demo

               Accuracy & precision estimates for various modes/devices.

               Newer approaches

Discussion and cautions.

 

Other IBF based liquid movement techniques, outside the box.

Nanoliter-sicles, making frozen charged spheres of liquid/s

Writing the word "picoliters" with pLs and IBF. The picoliter regime

The New Nanoliter/Microliter syringe (Patent Pending.)

Printing with monolithic LC columns for MALDI sample preparation

More morphing syringe pumps, peristaltic and other pumps into the nanoliter regime

Passive/active focusing. 

 

Summary.

            Why, where having the ability to manipulate nanoliters at your locale has merit.

Competitive techniques

Questions and answers

 

Handouts. Course Book, Article Reprints, Nanoliters

 

Course outline can be updated as and when we determine.

 

 

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